A SEM, EDX and XAS characterization of Ba(II)Fe(III) layered double hydroxides

D. Sranko; M. Sipiczki; E. G. Bajnoczi; M. Daranyi; A. Kukovecz; Z. Konya; Sophie Canton; Katarina Norén; P. Sipos; I. Palinko

doi:10.1016/j.molstruc.2010.10.004

A SEM, EDX and XAS characterization of Ba(II)Fe(III) layered double hydroxides

D. Sranko, M. Sipiczki, E. G. Bajnoczi, M. Daranyi, A. Kukovecz, Z. Konya, Sophie Canton, Katarina Norén, P. Sipos, I. Palinko

Research output: Chapter in Book/Report/Conference proceeding › Paper in conference proceeding › peer-review

Abstract

The structural characteristics of Ba-Fe double hydroxides were studied by various methods, such as scanning electron microscopy (SEM), energy dispersive X-ray (EDX) fluorescence and X-ray absorption spectroscopies (XAS). It was verified that under hyperalkaline conditions (using 10 M or 20 M NaOH solution for precipitating the substances) layered double hydroxides could be prepared and the structure collapsed on heat treatment at 523 K. Important structural parameters could also be obtained through the quantitative analysis of the XAS spectrum of Ba3Fe-LDH made using 20 M NaOH for precipitating the material. (C) 2010 Elsevier B.V. All rights reserved.

Original language	English
Title of host publication	Journal of Molecular Structure
Publisher	Elsevier
Pages	62-66
Volume	993
DOIs	https://doi.org/10.1016/j.molstruc.2010.10.004
Publication status	Published - 2011
Event	30th European Congress on Molecular Spectroscopy - Florence, Italy Duration: 2010 Aug 29 → 2010 Sept 3

Publication series

Name
Number	1-3
Volume	993
ISSN (Print)	0022-2860

Conference

Conference	30th European Congress on Molecular Spectroscopy
Country/Territory	Italy
City	Florence
Period	2010/08/29 → 2010/09/03

Bibliographical note

The information about affiliations in this record was updated in December 2015.
The record was previously connected to the following departments: Chemical Physics (S) (011001060), Biomedical Polymer Technology (013212010)

Subject classification (UKÄ)

Atom and Molecular Physics and Optics

Free keywords

BaFe-LDH
Scanning electron microscopy
Energy dispersive X-ray
analysis
X-ray absorption spectroscopy
Structural parameters

Access to Document

10.1016/j.molstruc.2010.10.004

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@inproceedings{b184a0092836449c865abd9b6ea1918c,

title = "A SEM, EDX and XAS characterization of Ba(II)Fe(III) layered double hydroxides",

abstract = "The structural characteristics of Ba-Fe double hydroxides were studied by various methods, such as scanning electron microscopy (SEM), energy dispersive X-ray (EDX) fluorescence and X-ray absorption spectroscopies (XAS). It was verified that under hyperalkaline conditions (using 10 M or 20 M NaOH solution for precipitating the substances) layered double hydroxides could be prepared and the structure collapsed on heat treatment at 523 K. Important structural parameters could also be obtained through the quantitative analysis of the XAS spectrum of Ba3Fe-LDH made using 20 M NaOH for precipitating the material. (C) 2010 Elsevier B.V. All rights reserved.",

keywords = "BaFe-LDH, Scanning electron microscopy, Energy dispersive X-ray, analysis, X-ray absorption spectroscopy, Structural parameters",

author = "D. Sranko and M. Sipiczki and Bajnoczi, {E. G.} and M. Daranyi and A. Kukovecz and Z. Konya and Sophie Canton and Katarina Nor{\'e}n and P. Sipos and I. Palinko",

note = "The information about affiliations in this record was updated in December 2015. The record was previously connected to the following departments: Chemical Physics (S) (011001060), Biomedical Polymer Technology (013212010); 30th European Congress on Molecular Spectroscopy ; Conference date: 29-08-2010 Through 03-09-2010",

year = "2011",

doi = "10.1016/j.molstruc.2010.10.004",

language = "English",

volume = "993",

publisher = "Elsevier",

number = "1-3",

pages = "62--66",

booktitle = "Journal of Molecular Structure",

address = "United States",

}

Sranko, D, Sipiczki, M, Bajnoczi, EG, Daranyi, M, Kukovecz, A, Konya, Z, Canton, S, Norén, K, Sipos, P & Palinko, I 2011, A SEM, EDX and XAS characterization of Ba(II)Fe(III) layered double hydroxides. in Journal of Molecular Structure. vol. 993, Elsevier, pp. 62-66, 30th European Congress on Molecular Spectroscopy, Florence, Italy, 2010/08/29. https://doi.org/10.1016/j.molstruc.2010.10.004

TY - GEN

T1 - A SEM, EDX and XAS characterization of Ba(II)Fe(III) layered double hydroxides

AU - Sranko, D.

AU - Sipiczki, M.

AU - Bajnoczi, E. G.

AU - Daranyi, M.

AU - Kukovecz, A.

AU - Konya, Z.

AU - Canton, Sophie

AU - Norén, Katarina

AU - Sipos, P.

AU - Palinko, I.

N1 - The information about affiliations in this record was updated in December 2015. The record was previously connected to the following departments: Chemical Physics (S) (011001060), Biomedical Polymer Technology (013212010)

PY - 2011

Y1 - 2011

N2 - The structural characteristics of Ba-Fe double hydroxides were studied by various methods, such as scanning electron microscopy (SEM), energy dispersive X-ray (EDX) fluorescence and X-ray absorption spectroscopies (XAS). It was verified that under hyperalkaline conditions (using 10 M or 20 M NaOH solution for precipitating the substances) layered double hydroxides could be prepared and the structure collapsed on heat treatment at 523 K. Important structural parameters could also be obtained through the quantitative analysis of the XAS spectrum of Ba3Fe-LDH made using 20 M NaOH for precipitating the material. (C) 2010 Elsevier B.V. All rights reserved.

AB - The structural characteristics of Ba-Fe double hydroxides were studied by various methods, such as scanning electron microscopy (SEM), energy dispersive X-ray (EDX) fluorescence and X-ray absorption spectroscopies (XAS). It was verified that under hyperalkaline conditions (using 10 M or 20 M NaOH solution for precipitating the substances) layered double hydroxides could be prepared and the structure collapsed on heat treatment at 523 K. Important structural parameters could also be obtained through the quantitative analysis of the XAS spectrum of Ba3Fe-LDH made using 20 M NaOH for precipitating the material. (C) 2010 Elsevier B.V. All rights reserved.

KW - BaFe-LDH

KW - Scanning electron microscopy

KW - Energy dispersive X-ray

KW - analysis

KW - X-ray absorption spectroscopy

KW - Structural parameters

U2 - 10.1016/j.molstruc.2010.10.004

DO - 10.1016/j.molstruc.2010.10.004

M3 - Paper in conference proceeding

VL - 993

SP - 62

EP - 66

BT - Journal of Molecular Structure

PB - Elsevier

T2 - 30th European Congress on Molecular Spectroscopy

Y2 - 29 August 2010 through 3 September 2010

ER -

A SEM, EDX and XAS characterization of Ba(II)Fe(III) layered double hydroxides

Abstract

Publication series

Conference

Bibliographical note

Subject classification (UKÄ)

Free keywords

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