An electrochemical cell for 2-dimensional surface optical reflectance during anodization and cyclic voltammetry

W. Linpé; G. S. Harlow; A. Larsson; G. Abbondanza; L. Rämisch; S. Pfaff; J. Zetterberg; J. Evertsson; E. Lundgren

doi:10.1063/1.5133905

An electrochemical cell for 2-dimensional surface optical reflectance during anodization and cyclic voltammetry

W. Linpé, G. S. Harlow, A. Larsson, G. Abbondanza, L. Rämisch, S. Pfaff, J. Zetterberg, J. Evertsson, E. Lundgren

Hydro Extruded Solutions AB

Research output: Contribution to journal › Article › peer-review

Abstract

We have developed an electrochemical cell for in situ 2-Dimensional Surface Optical Reflectance (2D-SOR) studies during anodization and cyclic voltammetry. The 2D-SOR signal was recorded from electrodes made of polycrystalline Al, Au(111), and Pt(100) single crystals. The changes can be followed at a video rate acquisition frequency of 200 Hz and demonstrate a strong contrast between oxidizing and reducing conditions. Good correlation between the 2D-SOR signal and the anodization conditions or the cyclic voltammetry current is also observed. The power of this approach is discussed, with a focus on applications in various fields of electrochemistry. The combination of 2D-SOR with other techniques, as well as its spatial resolution and sensitivity, has also been discussed.

Original language	English
Article number	044101
Journal	Review of Scientific Instruments
Volume	91
Issue number	4
DOIs	https://doi.org/10.1063/1.5133905
Publication status	Published - 2020

Subject classification (UKÄ)

Atom and Molecular Physics and Optics

Access to Document

10.1063/1.5133905

1 Doctoral Thesis (compilation)

Ordered arrays of low-dimensional Au and Pd: synthesis and in situ observations
Abbondanza, G., 2022, Lund University, Faculty of Science. 224 p.
Research output: Thesis › Doctoral Thesis (compilation)

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1 Finished

Combined techniques for studies of catalysis
Zetterberg, J.
Swedish Foundation for Strategic Research, SSF
2019/01/01 → 2023/12/31
Project: Research

Cite this

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title = "An electrochemical cell for 2-dimensional surface optical reflectance during anodization and cyclic voltammetry",

abstract = "We have developed an electrochemical cell for in situ 2-Dimensional Surface Optical Reflectance (2D-SOR) studies during anodization and cyclic voltammetry. The 2D-SOR signal was recorded from electrodes made of polycrystalline Al, Au(111), and Pt(100) single crystals. The changes can be followed at a video rate acquisition frequency of 200 Hz and demonstrate a strong contrast between oxidizing and reducing conditions. Good correlation between the 2D-SOR signal and the anodization conditions or the cyclic voltammetry current is also observed. The power of this approach is discussed, with a focus on applications in various fields of electrochemistry. The combination of 2D-SOR with other techniques, as well as its spatial resolution and sensitivity, has also been discussed.",

author = "W. Linp{\'e} and Harlow, {G. S.} and A. Larsson and G. Abbondanza and L. R{\"a}misch and S. Pfaff and J. Zetterberg and J. Evertsson and E. Lundgren",

year = "2020",

doi = "10.1063/1.5133905",

language = "English",

volume = "91",

journal = "Review of Scientific Instruments",

issn = "0034-6748",

publisher = "American Institute of Physics (AIP)",

number = "4",

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TY - JOUR

T1 - An electrochemical cell for 2-dimensional surface optical reflectance during anodization and cyclic voltammetry

AU - Linpé, W.

AU - Harlow, G. S.

AU - Larsson, A.

AU - Abbondanza, G.

AU - Rämisch, L.

AU - Pfaff, S.

AU - Zetterberg, J.

AU - Evertsson, J.

AU - Lundgren, E.

PY - 2020

Y1 - 2020

N2 - We have developed an electrochemical cell for in situ 2-Dimensional Surface Optical Reflectance (2D-SOR) studies during anodization and cyclic voltammetry. The 2D-SOR signal was recorded from electrodes made of polycrystalline Al, Au(111), and Pt(100) single crystals. The changes can be followed at a video rate acquisition frequency of 200 Hz and demonstrate a strong contrast between oxidizing and reducing conditions. Good correlation between the 2D-SOR signal and the anodization conditions or the cyclic voltammetry current is also observed. The power of this approach is discussed, with a focus on applications in various fields of electrochemistry. The combination of 2D-SOR with other techniques, as well as its spatial resolution and sensitivity, has also been discussed.

AB - We have developed an electrochemical cell for in situ 2-Dimensional Surface Optical Reflectance (2D-SOR) studies during anodization and cyclic voltammetry. The 2D-SOR signal was recorded from electrodes made of polycrystalline Al, Au(111), and Pt(100) single crystals. The changes can be followed at a video rate acquisition frequency of 200 Hz and demonstrate a strong contrast between oxidizing and reducing conditions. Good correlation between the 2D-SOR signal and the anodization conditions or the cyclic voltammetry current is also observed. The power of this approach is discussed, with a focus on applications in various fields of electrochemistry. The combination of 2D-SOR with other techniques, as well as its spatial resolution and sensitivity, has also been discussed.

U2 - 10.1063/1.5133905

DO - 10.1063/1.5133905

M3 - Article

C2 - 32357721

AN - SCOPUS:85083893703

SN - 0034-6748

VL - 91

JO - Review of Scientific Instruments

JF - Review of Scientific Instruments

IS - 4

M1 - 044101

ER -

An electrochemical cell for 2-dimensional surface optical reflectance during anodization and cyclic voltammetry

Abstract

Subject classification (UKÄ)

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Research output

Ordered arrays of low-dimensional Au and Pd: synthesis and in situ observations

Projects

Combined techniques for studies of catalysis

Cite this