Comprehensive comparison of classic Soxhlet extraction with Soxtec extraction, ultrasonication extraction, supercritical fluid extraction, microwave assisted extraction and accelerated solvent extraction for the determination of polychlorinated biphenyls in soil

Sune Sporring, S Bowadt, B Svensmark, Erland Björklund

Research output: Contribution to journalArticlepeer-review

131 Citations (SciVal)

Abstract

This paper compares the extraction effectiveness of six different commonly applied extraction techniques for the determination of PCBs in soil. The techniques included are Soxhlet, Soxtec, ultrasonication extraction, supercritical fluid extraction, microwave-assisted extraction and accelerated solvent extraction. For none of the techniques were the extraction conditions optimized, but instead the extraction parameters were based on the experience from previous successful investigation published by a number of research groups worldwide. In general, all extraction techniques were capable of producing accurate data for one native PCB contaminated soil diluted with another soil sample to obtain two concentration levels. It could therefore be concluded that any of the investigated techniques can be used with success if the extraction conditions applied are chosen wisely. (c) 2005 Published by Elsevier B.V.
Original languageEnglish
Pages (from-to)1-9
JournalJournal of Chromatography A
Volume1090
Issue number1-2
DOIs
Publication statusPublished - 2005

Bibliographical note

The information about affiliations in this record was updated in December 2015.
The record was previously connected to the following departments: Analytical Chemistry (S/LTH) (011001004)

Subject classification (UKÄ)

  • Analytical Chemistry

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