In-situ studies of the formation mechanism of SBA-15

Viveka Alfredsson; H. Amenitsch; Katarina Flodström; M. Linden; C. V. Teixeira; Håkan Wennerström; A. Sayari; M. Jaroniec

In-situ studies of the formation mechanism of SBA-15

Viveka Alfredsson, H. Amenitsch, Katarina Flodström, M. Linden, C. V. Teixeira, Håkan Wennerström, A. Sayari, M. Jaroniec

Physical Chemistry

Research output: Chapter in Book/Report/Conference proceeding › Paper in conference proceeding › peer-review

Abstract

The formation process of SBA-15 has been investigated by time resolved TEM, in-situ SAXS/SAXD and in-situ NMR. The synthesis was done at 35 degrees in acidic solution with tetramethylorthosilicate as the silica source and Pluronic P123 as the structure directing amphiphile. The initially formed silica-polymer composite consists of flocs of spherical micelles in a silica matrix. The micelles then coalesce forming rods that eventually pack into the ordered array of which SBA-15 consists.

Original language	English
Title of host publication	Nanoporous Materials IV, 156
Publisher	Elsevier
Pages	69-74
Volume	156
ISBN (Print)	0-444-51748-0
Publication status	Published - 2005

Publication series

Name
Volume	156

Subject classification (UKÄ)

Physical Chemistry (including Surface- and Colloid Chemistry)

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Cite this

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title = "In-situ studies of the formation mechanism of SBA-15",

abstract = "The formation process of SBA-15 has been investigated by time resolved TEM, in-situ SAXS/SAXD and in-situ NMR. The synthesis was done at 35 degrees in acidic solution with tetramethylorthosilicate as the silica source and Pluronic P123 as the structure directing amphiphile. The initially formed silica-polymer composite consists of flocs of spherical micelles in a silica matrix. The micelles then coalesce forming rods that eventually pack into the ordered array of which SBA-15 consists.",

author = "Viveka Alfredsson and H. Amenitsch and Katarina Flodstr{\"o}m and M. Linden and Teixeira, {C. V.} and H{\aa}kan Wennerstr{\"o}m and A. Sayari and M. Jaroniec",

year = "2005",

language = "English",

isbn = "0-444-51748-0",

volume = "156",

publisher = "Elsevier",

pages = "69--74",

booktitle = "Nanoporous Materials IV, 156",

address = "United States",

}

TY - GEN

T1 - In-situ studies of the formation mechanism of SBA-15

AU - Alfredsson, Viveka

AU - Amenitsch, H.

AU - Flodström, Katarina

AU - Linden, M.

AU - Teixeira, C. V.

AU - Wennerström, Håkan

AU - Sayari, A.

AU - Jaroniec, M.

PY - 2005

Y1 - 2005

N2 - The formation process of SBA-15 has been investigated by time resolved TEM, in-situ SAXS/SAXD and in-situ NMR. The synthesis was done at 35 degrees in acidic solution with tetramethylorthosilicate as the silica source and Pluronic P123 as the structure directing amphiphile. The initially formed silica-polymer composite consists of flocs of spherical micelles in a silica matrix. The micelles then coalesce forming rods that eventually pack into the ordered array of which SBA-15 consists.

AB - The formation process of SBA-15 has been investigated by time resolved TEM, in-situ SAXS/SAXD and in-situ NMR. The synthesis was done at 35 degrees in acidic solution with tetramethylorthosilicate as the silica source and Pluronic P123 as the structure directing amphiphile. The initially formed silica-polymer composite consists of flocs of spherical micelles in a silica matrix. The micelles then coalesce forming rods that eventually pack into the ordered array of which SBA-15 consists.

M3 - Paper in conference proceeding

SN - 0-444-51748-0

VL - 156

SP - 69

EP - 74

BT - Nanoporous Materials IV, 156

PB - Elsevier

ER -

In-situ studies of the formation mechanism of SBA-15

Abstract

Publication series

Subject classification (UKÄ)

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Cite this